Informasi Detil Paper

Judul: Sintesis 1-fenil-4-(3,4-dimetoksi fenil)-1-buten-3-on dari Eugenol
Penulis: Candra Y. Tahya, Hanoch J. Sohilait & Serly. J. Sekewael  || email:
Jurnal: Indonesian Journal of Chemical Research Vol. 2 no. 1 - hal. 124-130 Tahun 2014  [ MIPA ]
Keywords:  Eugenol, 1-phenyl-4-(3, 4-dimethoxy phenyl)-1-buten-3-one.
Abstract: The synthesis of 1-phenyl-4-(3’, 4’-dimethoxy phenyl)-1-buten-3-one from eugenol has been done through four reaction steps. The metilation of eugenol with dimethyl sulphate yields 81.81% of methyl eugenol. Oxymercuration-demercuration of methyl eugenol with mercury acetate yields 67.27% of methyl eugenyl alcohol. Oxidation of methyl eugenyl alcohol with pyridinium chloro chromate (PCC) yields 45.31% of methyl eugenyl ketone. Aldol condensation reaction of methyl eugenyl ketone with benzaldehide catalyzed by potasium hydroxyde yields 7.38% of 1-phenyl4-(3’,4’-dimethoxyphenyl)-1-buten-3-one. The purity of compounds was tested by GC and LC. The Elucidation of structure was analyzed by FTIR, GC-MS, LC-ESI-MS, and 1H-NMR.
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